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Citation: SUN Yuqiong, XIA Donghai, DONG Xinrong, LI Xia. A Simple Simultaneous Distillation/Solvent Extraction Method Coupled with Gas Chromatography-Mass Spectrometry for the Analysis of Volatile Oils of Illicium Verum[J]. Chinese Journal of Applied Chemistry, ;2015, 32(3): 356-361. doi: 10.11944/j.issn.1000-0518.2015.03.140196 shu

A Simple Simultaneous Distillation/Solvent Extraction Method Coupled with Gas Chromatography-Mass Spectrometry for the Analysis of Volatile Oils of Illicium Verum

1.
College of Science, Hu'nan Agricultural University, Changsha 410128, China

Corresponding author: LI Xia,
Received Date: 4 June 2014
Available Online: 29 October 2014
Fund Project: 湖南省科技厅基金项目(2011FJ6054) (2011FJ6054)

A simple simultaneous distillation and solvent extraction(SSDE) method was developed and had been applied for sample preparation of the gas chromatography-mass spectrometry(GC-MS) analysis of volatile components from Illicium Verum. The simple apparatus was composed of a round flask,a constant pressure dropping funnel and a condenser. The constituents of the volatile oil obtained by SSDE were compared with those obtained by hydrodistillation method(HD) followed by GC-MS analysis. In terms of GC-MS analysis of volatile oil,the relative standard deviation(RSD) values(n=3) of measured relative contents(>0.1%) of19 identified compounds are no more than 5.59%. The total content of above components is 98.84% of the volatile oil,in which there are 17 components in 89.5% content with RSD less than 5%. And the yield of volatile oil obtained by SSDE and HD is 7.30%(RSD 2.37%(n=5)) and 6.67%(RSD 5.26%(n=5)),respectively. These results indicate that SSDE is a simple,suitable method for the extraction of volatile oil from Illicium Verum.
- simultaneous distillation extraction,
- hydrodistillation,
- gas chromatography-mass spectrometry,
- volatile oil,
- Illicium Verum
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