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Citation: WU Qian, LIN Hua, LIU Ying, JIN Yong-Ri, LI Peng, LIU Wei-Jie, LI Xu-Wen. Ionic Liquid Ultrasonic-assisted Solid Phase Extraction of Four Kinds of Hosenkosides from Seeds of Impatiens balsamina L.[J]. Chinese Journal of Analytical Chemistry, ;2018, 46(6): 910-916. doi: 10.11895/j.issn.0253-3820.181062 shu

Ionic Liquid Ultrasonic-assisted Solid Phase Extraction of Four Kinds of Hosenkosides from Seeds of Impatiens balsamina L.

WU Qian ^1, ,
LIN Hua ² ,
LIU Ying ¹ ,
JIN Yong-Ri ¹ ,
LI Peng ¹ ,
LIU Wei-Jie ¹ ,
LI Xu-Wen ¹

1.
College of Chemistry, Jilin University, Changchun 130021, China;
2.
Clinical Laboratory of First Hospital, Jilin University, Changchun 130021, China

Received Date: 26 January 2018
Revised Date: 7 March 2018

A green, rapid and efficient method was developed for the extraction of 4 kinds of hosenkosides from the seeds of Impatiens balsamina L. The hosenkosides were extracted by ionic liquid, and then enriched by solid phase extraction. The effects of the kinds and volume of ionic liquid, pH value, ultrasonic time, solid phase extractant and eluent on the extraction fields were investigated and optimized. Under the optimum conditions, the recoveries of 4 kinds of hosenkosides were between 92.1% and 108.2%, the correlation coefficients were 0.9945-0.9975, and the detection limits were 1.8-4.5 μg/mL. The RSD values were all less than 3.9%. The experimental results showed that this method was fast, efficient, environmental protection. This study provided a reference for the extraction and enrichment of trace components in Chinese medicinal herbs.
- Ionic liquid,
- Solid phase extraction,
- Seeds of Impatiens balsamina L,
- Hosenkosides,
- Ultrasonic-assisted
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