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Citation: XIE Yue, ZHOU Cheng, TU Cong, ZHANG Zu-Liang, WANG Jian-Fei. Quantitative Determination of Ferulic Acid Content in Chrysanthemum Morifolium cv.(Chuju) Continuous Cropping Soil Using Near Infrared Spectroscopy[J]. Chinese Journal of Analytical Chemistry, ;2017, 45(3): 363-368. doi: 10.11895/j.issn.0253-3820.160773 shu

Quantitative Determination of Ferulic Acid Content in Chrysanthemum Morifolium cv.(Chuju) Continuous Cropping Soil Using Near Infrared Spectroscopy

XIE Yue ^1,2, ,
ZHOU Cheng ³ ,
TU Cong ² ,
ZHANG Zu-Liang ⁴ ,
WANG Jian-Fei ¹

1.
College of Resources and Environment, Anhui Science and Technology University, Fengyang 233100, China;
2.
Department of Plant Pathology, North Carolina State University, Raleigh, NC 27695, USA;
3.
College of Life Science, Anhui Science and Technology University, Fengyang 233100, China;
4.
Lu'an Institute for Food and Drug Control Center, Lu'an 237009, China

Received Date: 19 October 2016
Revised Date: 14 December 2016

Fund Project: This work was supported by the National Natural Science Foundation of China (No.21607002) and the Natural Science Foundation of Anhui Province, China (No.1508085QD74)

A near infrared spectroscopy (NIRS) method was used for rapid quality evaluation of ferulic acid content in chrysanthemum morifolium cv. (Chuju) continuous cropping soil. Standard leverage, studentized residual and Mahalanobis distance were calculated to eliminate abnormal samples. After the initial near infrared spectrum was treated by two second derivative and Norris smoothing filter noise, 6000-4000 cm^-1 wave number range and 7 factors were chosen for partial least squares (PLS) calibration model. The results showed that good correlation was presented between the calibration set/validation set and the values determined by high performance liquid chromatography, and the calibration correlation coefficient (R_c) and validation correlation coefficient (R_cv) were 0.9914 and 0.9935, respectively. Root mean square error of calibration (RMSEC), root mean square error of validation (RMSEP) and root mean square error of cross-validation (RMSECV) were 0.484, 0.539 and 0.615, respectively. This method was accurate, reliable, simple, rapid and nondestructive, and could be applied to the fast analysis for ferulic acid in continuous cropping soil.
- Near infrared transmittance spectroscopy,
- Continuous cropping soil,
- Chrysanthemum morifolium cv.(Chuju),
- Phenolic acids,
- Ferulic acid
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