Citation: LONG Tao, SHI Jian, BAO Ze-Min, Stephen W. J. Clement, ZHANG Yu-Hai, TIAN Di, LIU Dun-Yi. Influence of Edge Effect and X-Y Effect on Measurement Precision in Sensitive High Resolution Ion Microprobe IIe MC Oxygen Isotopes Analysis[J]. Chinese Journal of Analytical Chemistry, ;2015, 43(12): 1888-1894. doi: 10.11895/j.issn.0253-3820.150581 shu

Influence of Edge Effect and X-Y Effect on Measurement Precision in Sensitive High Resolution Ion Microprobe IIe MC Oxygen Isotopes Analysis

1.
¹ Department of Instrumentation & Electrical Engineering, Jilin University, Changchun 130026, China;

Corresponding author: LONG Tao,
Received Date: 21 July 2015
Available Online: 11 September 2015
Fund Project: 本文系国家重大科学仪器设备开发专项资助(No.2011YQ05006902) (No.2011YQ05006902)

Sensitive high resolution ion microprobe(SHRIMP) IIe MC has been widely used in the oxygen isotopes analysis of zircon, apatite, calcium carbonate, etc.. This study provides guidance for SHRIMP IIe MC high precision O-isotope analysis. We have established the secondary ion extraction structure of SIMION simulation model and discussed the cause and influencing factors of edge effect and X-Y effect in oxygen isotopes analysis. Higher δ¹⁸O precision can be reached by limiting O-isotope analysis position(the sample is located at the center of the mount within 10 mm diameter and the target surface roughness is less than 1μm). The internal precision of single spot of zircon δ¹⁸O is better than 0.15‰(1σ), with external precision better than 0.5%(95% confidence); the internal precision of the single analysis of Carbonate δ¹⁸O is better than 0.20‰(1σ), with external precision better than 0.6‰(95% confidence).
- Sensitive high resolution ion microprobe,
- Oxygen analysis,
- Edge effect,
- X-Y effect
1. [1]
  1 Compston W, Pidgeon R T. Nature, 1986, 321(6072):766-769
2. [2]
  2 Black L P, Kamo S L, Allen C M, Davis D W, Aleinikoff J N, Valley J W, Mundil R, Campbell I H, Korsch R J, Williams I S, Foudoulis C. Chem. Geol., 2004, 205(1-2):115-140
3. [3]
  3 Liu D, Jolliff B L, Zeigler R A, Korotev R L, Wan Y, Xie H, Zhang Y, Dong C, Wang W. Earth. Planetary Sci. Lett., 2012, 319-320:277-286
4. [4]
  4 White L T, Ireland T R. Chem. Geol., 2012, 306-307:78-91
5. [5]
  5 Ushikubo T, Williford K H, Farquhar J, Johnston D T, Van Kranendonk M J, Valley J W. Chem. Geol., 2014, 383:86-99
6. [6]
  6 Gao Y-Y, Li X-H, Griffin W L, O'Reilly S Y, Wang Y-F. Lithos, 2014, 192-195:180-191
7. [7]
  7 Ireland T R, Schram N, Holden P, Lanc P, Ávila J, Armstrong R, Amelin Y, Latimore A, Corrigan D, Clement S, Foster J J, Compston W. Inter. J. Mass Spectrom., 2014, 359:26-37
8. [8]
  8 Ickert R B, Hiess J, Williams I S, Holden P, Ireland T R, Lanc P, Schram N, Foster J J, Clement S W. Chem. Geol., 2008, 257(1-2):114-128
9. [9]
  9 Rubatto D, Putlitz B, Gauthiez-Putallaz L, Crépisson C, Buick I S, Zheng Y-F. Chem. Geol., 2014, 380:84-96
10. [10]
  10 Aubert M, Williams I S, Boljkovac K, Moffat I, Moncel M-H, Dufour E, Grün R. J. Archaeol. Sci., 2012, 39(10):3184-3194
11. [11]
  11 Trotter J A, Williams I S, Barnes C R, Lécuyer C, Nicoll R S. Science, 2008, 321(5888):550-554
12. [12]
  12 Martin L A J, Rubatto D, Crépisson C, Hermann J, Putlitz B, Vitale-Brovarone A. Chem. Geol., 2014, 374-375:25-36
13. [13]
  13 Iles K A, Hergt J M, Sircombe K N, Woodhead J D, Bodorkos S, Williams I S. Chem. Geol., 2015, 402:140-152
14. [14]
  14 Treble P, Schmitt A, Edwards R, McKeegan K, Harrison T, Grove M, Cheng H, Wang Y. Chem. Geol., 2007, 238(3-4):197-212
15. [15]
  15 Kita N T, Ushikubo T, Fu B, Valley J W. Chem. Geol., 2009, 264(1-4):43-57
16. [16]
  16 Whitehouse M J, Nemchin A A. Chem. Geol., 2009, 261(1-2):32-42
17. [17]
  17 Matsuda H. Inter. J. Mass Spectrom. Ion Phy., 1974, 14(2):219-233
18. [18]
  18 Clement S W J, Compston W, Newstead G. Proceedings of the International Conference on SIMS and Ion Microprobes, Muenster,Germany(unpublished ms.). 1977
19. [19]
  19 ClementS W C, In:Benninghoven A, Evans C A, McKeegan K D, Storms H A,Werner H W.(Eds.). Secondary Ion Mass Spectrometry, SIMS VII. John Wiley & Sons, 1990:815-819
20. [20]
  20 Ireland T R, Clement S, Compston W, Foster J J, Holden P, Jenkins B, Lanc P, Schram N, Williams I S. Australian J. Earth Sci., 2008, 55(6):937-954
21. [21]
  21 Black L P, Kamo S L, Allen C M, Aleinikoff J N, Davis D W, Korsch R J, Foudoulis C. Chem. Geol., 2003, 200(1-2):155-170
22. [22]
  22 Nasdala L, Hofmeister W, Mattinson J, Doerr W, Corfu F, Reiners P W, Kronz A, Norberg N, Kroener A. Geochim. Et Cosmochim. Acta, 2007, 71:A705
23. [23]
  23 Nasdala L, Hofmeister W, Norberg N, Mattinson J M, Corfu F, Doerr W, Kamo S L, Kennedy A K, Kronz A, Reiners P W, Frei D, Kosler J, Wan Y S, Goetze J, Haeger T, Kroener A, Valley J W. Geostand. Geoanal. Res., 2008, 32(3):247-265
24. [24]
  24 Wiedenbeck M, Hanchar J M, Peck W H, Sylvester P, Valley J, Whitehouse M, Kronz A, Morishita Y, Nasdala L, Fiebig J, Franchi I, Girard J P, Greenwood R C, Hinton R, Kita N, Mason P R D, Norman M, Ogasawara M, Piccoli P M, Rhede D, Satoh H, Schulz-Dobrick B, Skår O, Spicuzza M J, Terada K, Tindle A, Togashi S, Vennemann T, Xie Q, Zheng Y F. Geostand. Geoanal. Res., 2004, 28(1):9-39
25. [25]
  25 Eiler J M, Graham C, Valley J W. Chem. Geol., 1997, 138(3-4):221-244
26. [26]
  26 Schuhmacher M, Fernandes F, de Chambost E. App. Surf. Sci., 2004, 231-232:878-882
1. [1]
  Runze Xu , Rui Liu . U-Pb Dating in the Age of Dinosaurs. University Chemistry, 2024, 39(9): 243-247. doi: 10.12461/PKU.DXHX202404083
2. [2]
  Yaling Chen . Basic Theory and Competitive Exam Analysis of Dynamic Isotope Effect. University Chemistry, 2024, 39(8): 403-410. doi: 10.3866/PKU.DXHX202311093
3. [3]
  Wenwen Zhang , Peichao Zhang , Conghao Gai , Xiaoyun Chai , Yan Zou , Qingjie Zhao . Unveiling Kinetics at Natural Abundance: ¹³C NMR Isotope Effect Experiments. University Chemistry, 2025, 40(10): 203-207. doi: 10.12461/PKU.DXHX202411076
4. [4]
  Xingyuan Lu , Yutao Yao , Junjing Gu , Peifeng Su . Energy Decomposition Analysis and Its Application in the Many-Body Effect of Water Clusters. University Chemistry, 2025, 40(3): 100-107. doi: 10.12461/PKU.DXHX202405074
5. [5]
  Kexin Dong , Chuqi Shen , Ruyu Yan , Yanping Liu , Chunqiang Zhuang , Shijie Li . Integration of Plasmonic Effect and S-Scheme Heterojunction into Ag/Ag₃PO₄/C₃N₅ Photocatalyst for Boosted Photocatalytic Levofloxacin Degradation. Acta Physico-Chimica Sinica, 2024, 40(10): 2310013-0. doi: 10.3866/PKU.WHXB202310013
6. [6]
  Junyu Peng , Feng Wang , Hongmei Yuan , Xiaoli Sun . Exploration of the “Sheep-Flock Effect” Teaching Model Based on Dual Preview: Taking Instrumental Analysis Experiment Courses in Local Universities as an Example. University Chemistry, 2025, 40(9): 310-317. doi: 10.12461/PKU.DXHX202412098
7. [7]
  Xiaotian ZHU , Fangding HUANG , Wenchang ZHU , Jianqing ZHAO . Layered oxide cathode for sodium-ion batteries: Surface and interface modification and suppressed gas generation effect. Chinese Journal of Inorganic Chemistry, 2025, 41(2): 254-266. doi: 10.11862/CJIC.20240260
8. [8]
  Zongyuan Chen , ChunSheng Shi , Yiwen Li , Ganlin Zu , Qiang Jin , Haishan Wang , Fujun Wang , Dekun Yan , Zhijun Guo , Wangsuo Wu . Measurement of Uranium Isotopes in Environmental Water Samples by Alpha-Spectroscopy: Design of an Undergraduate Radiochemistry Experiment. University Chemistry, 2025, 40(4): 353-358. doi: 10.12461/PKU.DXHX202406103
9. [9]
  Chao Liu , Huan Yu , Jiaming Li , Xi Yu , Zhuangzhi Yu , Yuxi Song , Feng Zhang , Qinfang Zhang , Zhigang Zou . 具有光热效应的多级Ti₃C₂/Bi₁₂O₁₇Br₂肖特基异质结简单合成及其太阳能驱动抗生素光降解的研究. Acta Physico-Chimica Sinica, 2025, 41(7): 100075-0. doi: 10.1016/j.actphy.2025.100075
10. [10]
  Tieping CAO , Yuejun LI , Dawei SUN . Surface plasmon resonance effect enhanced photocatalytic CO₂ reduction performance of S-scheme Bi₂S₃/TiO₂ heterojunction. Chinese Journal of Inorganic Chemistry, 2025, 41(5): 903-912. doi: 10.11862/CJIC.20240366
11. [11]
  Shipeng WANG , Shangyu XIE , Luxian LIANG , Xuehong WANG , Jie WEI , Deqiang WANG . Piezoelectric effect of Mn, Bi co-doped sodium niobate for promoting cell proliferation and bacteriostasis. Chinese Journal of Inorganic Chemistry, 2024, 40(10): 1919-1931. doi: 10.11862/CJIC.20240094
12. [12]
  YanYuan Jia , Rong Rong , Jie Liu , Jing Guo , GuoYu Jiang , Shuo Guo . Unity is Strength, and Independence Shines: A Science Popularization Experiment on AIE and ACQ Effects. University Chemistry, 2024, 39(9): 349-358. doi: 10.12461/PKU.DXHX202402035
13. [13]
  Supin Zhao , Jing Xie . Understanding the Vibrational Stark Effect of Water Molecules Using Quantum Chemistry Calculations. University Chemistry, 2025, 40(3): 178-185. doi: 10.12461/PKU.DXHX202406024
14. [14]
  Yaqin Zheng , Lian Zhuo , Meng Li , Chunying Rong . Enhancing Understanding of the Electronic Effect of Substituents on Benzene Rings Using Quantum Chemistry Calculations. University Chemistry, 2025, 40(3): 193-198. doi: 10.12461/PKU.DXHX202406119
15. [15]
  Xinyi Fan , Wancai Shi , Zhenyu Sun . 甲烷——温室效应中的“隐形杀手”与绿色转机. University Chemistry, 2025, 40(11): 1-10. doi: 10.12461/PKU.DXHX202412060
16. [16]
  Ying Zhang , Fang Ge , Zhimin Luo . AI-Driven Biochemical Teaching Research: Predicting the Functional Effects of Gene Mutations. University Chemistry, 2025, 40(3): 277-284. doi: 10.12461/PKU.DXHX202412104
17. [17]
  Lei Feng , Ze-Min Zhu , Ying Yang , Zongbin He , Jiafeng Zou , Man-Bo Li , Yan Zhao , Zhikun Wu . Long-Pursued Structure of Au₂₃(S-Adm)₁₆ and the Unexpected Doping Effects. Acta Physico-Chimica Sinica, 2024, 40(5): 2305029-0. doi: 10.3866/PKU.WHXB202305029
18. [18]
  Jiaxi Xu , Yuan Ma . Influence of Hyperconjugation on the Stability and Stable Conformation of Ethane, Hydrazine, and Hydrogen Peroxide. University Chemistry, 2024, 39(11): 374-377. doi: 10.3866/PKU.DXHX202402049
19. [19]
  Cheng PENG , Jianwei WEI , Yating CHEN , Nan HU , Hui ZENG . First principles investigation about interference effects of electronic and optical properties of inorganic and lead-free perovskite Cs₃Bi₂X₉ (X=Cl, Br, I). Chinese Journal of Inorganic Chemistry, 2024, 40(3): 555-560. doi: 10.11862/CJIC.20230282
20. [20]
  Weikang Wang , Yadong Wu , Jianjun Zhang , Kai Meng , Jinhe Li , Lele Wang , Qinqin Liu . Green H₂O₂ synthesis via melamine-foam supported S-scheme Cd_0.5Zn_0.5In₂S₄/S-doped carbon nitride heterojunction: synergistic interfacial charge transfer and local photothermal effect. Acta Physico-Chimica Sinica, 2025, 41(8): 100093-0. doi: 10.1016/j.actphy.2025.100093

Get Citation

PDF

XML

Metrics

PDF Downloads(0)
Abstract views(512)
HTML views(26)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142