Citation: Jing REN, Ruikui YAN, Xiaoli CHEN, Huali CUI, Hua YANG, Jijiang WANG. Synthesis and fluorescence sensing of a highly sensitive and multi-response cadmium coordination polymer[J]. Chinese Journal of Inorganic Chemistry, ;2025, 41(3): 574-586. doi: 10.11862/CJIC.20240287 shu

Synthesis and fluorescence sensing of a highly sensitive and multi-response cadmium coordination polymer

School of Chemistry and Chemical Engineering, Shaanxi Key Laboratory of Chemical Reaction Engineering, Laboratory of New Energy & New Function Materials, Yan′an University, Yan′an, Shaanxi 716000, China

Corresponding author: Xiaoli CHEN, chenxiaoli003@163.com
Received Date: 30 July 2024
Revised Date: 18 December 2024

Figures(7)

A coordination polymer {[Cd(H₂dpa)(bpy)]·3H₂O}_n (Cd-CP) was designed and hydrothermal synthesized based on 4-(2, 4-dicarboxyphenoxy) phthalic acid (H₄dpa), 2, 2′-bipyridine (bpy) and Cd(NO₃)₂·4H₂O. The structure was characterized by single-crystal X-ray diffraction, powder X-ray diffraction, elemental analysis, and infrared spectroscopy. Cd-CP belongs to the monoclinic crystal system with the P2₁/c space group and performs in a 1D double-chain structure. The adjacent double chains further form a 3D supramolecular network structure through hydrogen bonding. Thermogravimetric analysis shows that Cd-CP has good thermal stability. Fluorescence analysis showed that Cd-CP had good choosing selectively and was sensitive to metal ions (Fe³⁺ and Zn²⁺), 2, 4, 6-trinitrophenylhydrazine (TRI), and pyrimethanil (Pth). Interestingly, when Cd-CP was used for fluorescence detection of metal ions, it was found to have a fluorescence quenching effect on Fe³⁺ but had an obvious enhancement effect on Zn²⁺. Therefore, we designed an "on-off-on" logic gate. In addition, the mechanism of fluorescence sensing has been deeply explored.
- coordination polymer,
- 4-(2, 4-dicarboxyphenoxy) phthalic acid,
- fluorescence sensing,
- logic gate
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