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Citation: Fei-Xiang WANG, Yong SHEN, Hong PAN, Li-Hui XU. Preparation and wave-absorbing properties of flower-like Zn-MOF-derived carbon@MoS2 composites[J]. Chinese Journal of Inorganic Chemistry, ;2023, 39(5): 830-840. doi: 10.11862/CJIC.2023.046 shu

Preparation and wave-absorbing properties of flower-like Zn-MOF-derived carbon@MoS2 composites

  • College of Textile and Clothing, Shanghai University of Engineering and Technology, Shanghai 201620, China

  • Corresponding author: Yong SHEN, shenyong@sues.edu.cn
  • Received Date: 24 October 2022
    Revised Date: 15 March 2023

Figures(6)

  • The polyhedral structure of Zn-MOF (MOF: metal-organic framework) was synthesized by the coordination of zinc nitrate hexahydrate and 2-methylimidazole. The Zn-MOF was calcined at high temperatures in a nitrogen atmosphere to prepare nanoporous carbon materials. In the process of preparation of flower-like MoS2 by solvothermal reaction, the Zn-MOF-derived nanoporous carbon was introduced and combined with flower-like MoS2 through self-assembly to prepare flower-like Zn-MOF-derived carbon@MoS2 composite absorbing material with regular and ordered structure. A series of characterization and performance tests were carried out to study the physical properties and absorbing properties of the composites. The particle size of polyhedral Zn-MOF-derived nanoporous carbon was 80 nm and encased in 1 μm flower-like MoS2. With the increase of the amount of Zn-MOF-derived carbon, the electromagnetic wave absorption performance of the flower-like Zn-MOF-derived carbon@MoS2 composites firstly increased and then decreased. Based on the high porosity and large specific surface area of Zn-MOF-derived porous carbon and the flower-like structure of MoS2, the electromagnetic wave was reflected and scattered many times, and there was a strong polarization effect, good impedance matching, and synergistic effect between MoS2 and Zn-MOF-derived carbon. When the additional amount (mass fraction) of flower-like Zn-MOF-derived carbon@MoS2 in paraffin was 25%, the frequency was 9.28 GHz, the matching thickness was 3 mm, and the effective absorption bandwidth was 3.04 GHz, the optimal reflection loss reached -49.68 dB, showing excellent electromagnetic wave absorption performance.
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