Citation: Ken-Ken LI, Song-Lei WANG, Rui-Ming LUO, Liang MA, Li LIU, Pei-Yuan WEI, Ye ZHANG. Nickel Bicarbonate Nanoparticles Loaded on Carbon Paper for Enzyme-Free Glucose Electrochemical Sensor[J]. Chinese Journal of Inorganic Chemistry, ;2021, 37(11): 2002-2010. doi: 10.11862/CJIC.2021.239 shu

Nickel Bicarbonate Nanoparticles Loaded on Carbon Paper for Enzyme-Free Glucose Electrochemical Sensor

College of Food and Wine, Ningxia University, Yinchuan 750021, China

Corresponding author: Song-Lei WANG, wangsonglei163@126.com
Received Date: 26 April 2021
Revised Date: 30 August 2021

Figures(8)

Nickel bicarbonate nanoparticles were grown in situ on carbon paper by one-step hydrothermal method. Powder X-ray diffraction and scanning electron microscopy were used to characterize the structure and morphology of the material. It was found that when pure phase Ni(HCO₃)₂ was loaded on carbon paper, it could provide more catalytically active sites which is beneficial to electron transport and catalytic reaction. Cyclic voltammetry and timecurrent response curves showed that the detection limit of the electrode was 0.98 μmol·L^-1, the linear range was 2.95-1.02 mmol·L^-1, and the sensitivity was 935 μA·L·mmol^-1·cm^-2. At the same time, it also exhibited excellent specificity and stability. In addition, the sensor can realize the rapid detection of glucose in dairy products. These results show that the synergistic effect of transition metal and conductive substrate can enhance the overall conductivity and catalytic performance of the composite material.
- enzyme-free sensor,
- carbon paper,
- nickel bicarbonate,
- cyclic voltammetry,
- glucose
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