Citation: MENG Shuo, ZHAO Meng-Jie, WEI Qin-Lei, ZOU Xiang-Yu, ZHANG Hong-Bo, SU Chun-Hui. Preparation and Characterization of Er³⁺-Yb³⁺ Co-doped SiO₂-SrO-NaF Glass Ceramics[J]. Chinese Journal of Inorganic Chemistry, ;2017, 33(9): 1505-1509. doi: 10.11862/CJIC.2017.204 shu

Preparation and Characterization of Er³⁺-Yb³⁺ Co-doped SiO₂-SrO-NaF Glass Ceramics

1.
College of Chemical and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022, China
2.
Changchun Normal University, Changchun 130032, China

Corresponding author: ZHANG Hong-Bo, zhb5388460@126.com SU Chun-Hui,
Received Date: 14 April 2017
Revised Date: 20 July 2017

Figures(6)

Er³⁺-Yb³⁺ co-doped transparent oxyfluoride glass ceramics containing SrF₂ crystals were successfully synthesized using a high temperature melting quenching method. The structure, morphology and luminescent properties of the samples were measured and characterized by DSC, XRD, SEM and fluorescence spectra. The results show that the optimum heat treatment temperature is 620℃, and the optimum heat treatment tine is 2 h. The effect of Er³⁺-Yb³⁺ co-doped glass ceramics with different doping concentrations of Yb³⁺ on the up-conversion luminescence properties was discussed. The optimum doping concentration ratio of Er³⁺-Yb³⁺ is 1:7. Bright green light (522, 540 nm) and weak red light (656 nm) were observed in the luminescence spectra. The energy transfer process between Er³⁺ and Yb³⁺ was discussed.
- SrF₂,
- glass ceramics,
- Er³⁺-Yb³⁺ co-doped,
- up-conversion
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沈阳化工大学材料科学与工程学院沈阳 110142

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通讯作者: 陈斌, bchen63@163.com

Preparation and Characterization of Er³⁺-Yb³⁺ Co-doped SiO₂-SrO-NaF Glass Ceramics