Citation: ZHENG Long-Zhen, KANG Xiao-Wei, JI Yi, ZOU Zhi-Jun, WANG Yi-Min, CHEN Ji-Fang. Preparation of Ag/ZIF-90 Self-Assembled Membrane and Its High SERS Performance[J]. Chinese Journal of Inorganic Chemistry, ;2015, (3): 465-471. doi: 10.11862/CJIC.2015.079 shu

Preparation of Ag/ZIF-90 Self-Assembled Membrane and Its High SERS Performance

1.
School of Sciences, East China Jiao Tong University, Nanchang 330013, China

Corresponding author: ZHENG Long-Zhen,
Received Date: 16 August 2014
Available Online: 7 November 2014
Fund Project: 国家自然科学基金(No.21163007, 21165009, 21465011) (No.21163007, 21165009, 21465011) 江西省主要学科学术和技术带头人计划(No.20133BCB22007) (No.20133BCB22007)江西省自然科学基金(No.20132BAB203012)资助项目。 (No.20132BAB203012)

Zeolitic imidazolate framework-90 (ZIF-90) sol-gel and ZIF-90 crystal membrane were prepared. Then silver nanoparticles(Ag NPs) were hosted in the ZIF-90 sol-gel or on the ZIF-90 crystal membrane to form Ag@ZIF-90 composite or Ag/ZIF-90 self-assembled membrane. The Ag@ZIF-90 composite and Ag/ZIF-90 self-assembled membrane were characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) and scanning electron microscopy (SEM) to show their morphorogies and structural features. Rhodamine 6G (R 6G) was used as a detection molecule to test the surface enhanced Raman scattering (SERS) performance of Ag@ZIF-90 composite and Ag/ZIF-90 self-assembled membrane. The SERS signal of R 6G on Ag/ZIF-90 self-assembled membrane was much higher than that on Ag@ZIF-90 composite and the background peak of ZIF-90 did not affect the SERS detection. The Ag/ZIF-90 self-assembled membrane was a promising active SERS substrate, which can be applied in the trace detection of pesticide residue.
- zeolitic imidazolate frameworks;Ag@ZIF-90 composite;Ag/ZIF-90 self-assembled membrane; surface enhanced Raman scattering (SERS)
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沈阳化工大学材料科学与工程学院沈阳 110142