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Citation: YI Xi-Bin, WANG Xiu-Chun, ZHANG Jing, MA Jie, LIU Shuo, SHEN Xiao-Dong, CUI Sheng. Synthesis and Characterization of SiO2 Composite Aerogels Enhanced by the Self Growing Nano-Fibers[J]. Chinese Journal of Inorganic Chemistry, ;2014, 30(3): 603-608. doi: 10.11862/CJIC.2014.103 shu

Synthesis and Characterization of SiO2 Composite Aerogels Enhanced by the Self Growing Nano-Fibers

  • 1.

    1 Institute of the New Material Research, Shandong Academy of Sciences, Key Laboratory for Adhesion & Sealing Materials of Shandong Province, Jinan 250014, China;

  • Received Date: 11 September 2013
    Available Online: 30 October 2013

    Fund Project: 国家安全重大基础研究(No.613120020020202) (No.613120020020202)山东省优秀中青年科学家科研奖励基金计划(No.BS2013CL038) (No.BS2013CL038)山东省自然科学基金 (No.ZR2011BL021) (No.ZR2011BL021)材料化学工程国家重点实验室开放课题基金(No.KL12-07) (No.KL12-07)山东省科技发展计划(NO.2013YD02046) (NO.2013YD02046)山东省科学院 青年基金项目(NO.2013QN019)资助项目。 (NO.2013QN019)

  • The SiO2 composite aerogels enhanced by the self growing nano-fibers were prepared using sol-gel techniques and supercritical fluid drying, and converted to the high-strength composite aerogels after 1 200 ℃ high temperature heat treatment process. The structures and properties of composite aerogels were analyzed by means of SEM, TEM, XRD, TG, BET, and the compressive strengths and the true density were also measured. The experimental results showed that the as-synthesized ZrOX/SiO2 composite aerogels exhibited well-proportioned multihole network structure, and the Zirconium oxide nano-fibers alternated in the composite aerogels by the chemical bond. The mechanical strength and the insulation properties were improved evidently. The specific surface area, the compressive strengths and the true density of the ZrOX/SiO2 composite aerogels after 1 200 ℃ high temperature heat treatment process were 827.22 m2·g-1, 9.68 MPa, 0.23 g·cm-3, respectively.
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    1. [1]

      [1] Pérez-Caballero F, Peikolainen A L, Uibu M, et al. Micropor.Mesopor. Mater., 2008,108(1):230-236

    2. [2]

      [2] LIU Ning(刘宁). Chinese J. Inorg. Chem. (无机化学学报),2013,29(3):551-556

    3. [3]

      [3] Gorle B S K, Smirnova I, Dragan M, et al. J. Supercrit. Fluids, 2008,44:78-84

    4. [4]

      [4] GAO Qing-Fu(高庆福), ZHANG Chang-Rui(张长瑞), FENG Jian(冯坚), et al. Chinese J. Inorg. Chem. (无机化学学报), 2008,24(9):1456-1460

    5. [5]

      [5] Cui S, Cheng W W, Shen X D, et al. Energy Environ. Sci., 2011,4(6):2070-2074

    6. [6]

      [6] FENG Jian(冯坚), FENG Jun-Zong(冯军宗), JIANG Yong-Gang(姜勇刚). Aerosp. Mater. Technol. (宇航材料工艺),2012,42(2):42-46

    7. [7]

      [7] Zhong Y, Kong Y, Shen X, et al. Micropor. Mesopor. Mater.,2013,172:182-189

    8. [8]

      [8] ZHONG Ya(仲亚), KONG Yong(孔勇), SHEN Xiao-Dong(沈晓冬), et al. J. Nanjing Univ. Tech.(南京工业大学学报),2012,34(5):26-29

    9. [9]

      [9] WU Li-Na(吴丽娜), HUANG Yu-Dong(黄玉东), WANG Zhi-Jiang(王志江), et al. Acta Phys.-Chim. Sin. (物理化学学报), 2010,26(6):1717-1721

    10. [10]

      [10] YANG Jie(杨杰), LI Shu-Kui(李树奎), WANG Fu-Chi (王富耻), et al. J. Beijing Inst. Tech.(北京工业大学学报), 2010,30(6):746-756

    11. [11]

      [11] ZHAO Nan(赵南), FENG Jian(冯坚), JIANG Yong-Gang (姜勇刚), et al. J. Chin. Ceram. Soc.(硅酸盐学报), 2012,40 (10):1473-1477

    12. [12]

      [12] FENG Jian(冯坚), GAO Qing-Fu(高庆福), FENG Jun-Zong (冯军宗), et al. J. National Univ. Defense Tech.(国防科技 大学学报), 2010,32(1):40-44

    13. [13]

      [13] WU Hui-Jun(吴会军), PENG Cheng(彭程), DING Yun-Fei(丁云飞), et al. J. Guangzhou Univ.(广州大学学报), 2012,6:32-37

    14. [14]

      [14] ZHANG He-Xin(张贺新), HE Xiao-Dong(赫晓东), LI Yao (李垚). Rare Met. Mater. Eng.(稀有金属材料工程), 2007,36 (1):567-569

    15. [15]

      [15] Skaltsas T, Avgouropoulos G, Tasis D. Micropor. Mesopor. Mater., 2011,143(2):451-457

    16. [16]

      [16] ZHONG Ya(仲亚), ZHANG Jun-Jun(张君君), SHEN Xiao-Dong(沈晓冬), et al. Chinese J. Inorg. Chem. (无机化学学 报), 2013,29(2):319-325

    17. [17]

      [17] Kong Y, Zhong Y, Shen X D, et al. Non-Cryst. Solids, 2012, 358(23):3150-3155

    18. [18]

      [18] KONG Yong(孔勇), SHEN Xiao-Dong(沈晓冬), CUI Sheng (崔升), et al. Chinese J. Inorg. Chem. (无机化学学报), 2012,28(10):2071-2076

    19. [19]

      [19] Kim G S, Hyun S H. J. Mater. Sci., 2003,38(9):1961-1966

    20. [20]

      [20] WANG Dong-Dong(王冬冬), WANG Gang(王刚), SUN Xiao-Fei(孙小飞), et al. Chinese J. Inorg. Chem. (无机化学 学报), 2012,28(3):491-494

    21. [21]

      [21] FENG Jian(冯坚), GAO Qing-Fu(高庆福), WU Wei(武纬), et al. Chinese J. Inorg. Chem. (无机化学学报), 2009,25 (10):1758-1763

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