Citation: Yong Zhao, Guo-min Li, Xue-min Dai, Fang-fang Liu, Zhi-xin Dong, Xue-peng Qiu. AO-resistant Properties of Polyimide Fibers Containing Phosphorous Groups in Main Chains[J]. Chinese Journal of Polymer Science, ;2016, 34(12): 1469-1478. doi: 10.1007/s10118-016-1864-7 shu

AO-resistant Properties of Polyimide Fibers Containing Phosphorous Groups in Main Chains

a.
Polymer Composites Engineering Laboratory, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China
b.
University of Chinese Academy of Sciences, Beijing 100049, China

Corresponding author: Zhi-xin Dong, zxdong@ciac.ac.cn Xue-peng Qiu, xp_q@ciac.ac.cn
Received Date: 23 June 2016
Revised Date: 29 August 2016
Accepted Date: 30 August 2016

Fund Project: National Basic Research Program of China 973 Program, No. 2014CB643604the National Natural Science Foundation of China 51373164

A series of polyimide fibers containing phosphorus element derived from (3-aminophenyl) methyl phosphine oxide (DAMPO) diamine was exposed to an artificial atomic oxygen environment which simulated the space environment in low earth orbit (LEO). The mass loss, surface morphology, chemical composition, and mechanical properties of the fibers before and after atomic oxygen (AO) exposure were compared in detail with a blank sample. Results showed that the phosphor-containing fibers demonstrated lower mass change and less tensile strength reduction. SEM results showed that the fibers with phosphorous element had relatively dense surface after AO exposure. Meanwhile, XPS results indicated that a passivated phosphate layer, which could protect the following under-layer from attacking by AO, was formed on the surface of the fibers. These results indicated that the incorporation of diamine (DAMPO) into the main chains could protect the fibers for avoiding further erosion from AO exposure. Hence, the phosphor-containing PI fibers exhibits potential application in space fields.
- Atomic oxygen,
- Phosphorous,
- Polyimide Fibers,
- LEO environment
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