引用本文:
Zhi Bin XU, Zong Ru GUO. An Abnormal Reaction of N-(2,4-dinitrophenyl)-L-proline with Thionyl Chloride[J]. Chinese Chemical Letters,
2003, 14(2): 133-134.
Citation: Zhi Bin XU, Zong Ru GUO. An Abnormal Reaction of N-(2,4-dinitrophenyl)-L-proline with Thionyl Chloride[J]. Chinese Chemical Letters, 2003, 14(2): 133-134.
Citation: Zhi Bin XU, Zong Ru GUO. An Abnormal Reaction of N-(2,4-dinitrophenyl)-L-proline with Thionyl Chloride[J]. Chinese Chemical Letters, 2003, 14(2): 133-134.
An Abnormal Reaction of N-(2,4-dinitrophenyl)-L-proline with Thionyl Chloride
摘要:
N-(2,4-Dinitrophenyl)-4-amino-n-butyl aldehyde 3 was obtained with high yield of 80% when N-(2,4-dinitrophenyl)-L-proline 1 reacted with SOCl2 at room temperature.However, the anticipated product N-(2,4-dinitrophenyl)-tetrahydropyrrolyl-2-(4-methylthiophenyl) ketone 2 did not be produced.The mechanism was discussed in this article.
English
An Abnormal Reaction of N-(2,4-dinitrophenyl)-L-proline with Thionyl Chloride
Abstract:
N-(2,4-Dinitrophenyl)-4-amino-n-butyl aldehyde 3 was obtained with high yield of 80% when N-(2,4-dinitrophenyl)-L-proline 1 reacted with SOCl2 at room temperature.However, the anticipated product N-(2,4-dinitrophenyl)-tetrahydropyrrolyl-2-(4-methylthiophenyl) ketone 2 did not be produced.The mechanism was discussed in this article.
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