引用本文:
Xin LIU, Rut Lian SHAO, Run Qiu HUANG. An Efficient Method for the Synthesis of Aliphatic α-Organothio Aldoximes[J]. Chinese Chemical Letters,
1999, 10(2): 97-98.
Citation: Xin LIU, Rut Lian SHAO, Run Qiu HUANG. An Efficient Method for the Synthesis of Aliphatic α-Organothio Aldoximes[J]. Chinese Chemical Letters, 1999, 10(2): 97-98.
Citation: Xin LIU, Rut Lian SHAO, Run Qiu HUANG. An Efficient Method for the Synthesis of Aliphatic α-Organothio Aldoximes[J]. Chinese Chemical Letters, 1999, 10(2): 97-98.
An Efficient Method for the Synthesis of Aliphatic α-Organothio Aldoximes
摘要:
A new and simple procedure for the synthesis of aliphatic α-organothio aldoximes was reported. The aliphatic aldoxime was chlorinated by t-BuOCl, the resulting hydroxime acid chloride was treated with triethylamine and alkyl mercaptan in a one pot procedure to get the target compounds. The method is very efficient with high yield and good purity.
English
An Efficient Method for the Synthesis of Aliphatic α-Organothio Aldoximes
Abstract:
A new and simple procedure for the synthesis of aliphatic α-organothio aldoximes was reported. The aliphatic aldoxime was chlorinated by t-BuOCl, the resulting hydroxime acid chloride was treated with triethylamine and alkyl mercaptan in a one pot procedure to get the target compounds. The method is very efficient with high yield and good purity.
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Key words:
- Aliphatic α-organothio aldoximes
- / α-chlorination
- / t-butyl hypochlorite
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