引用本文:
王福泉, 王毅, 王祥云. 关于十二硼烷二钠盐的合成[J]. 应用化学,
1998, 15(5): 111-112.
Citation: Wang Fuquan, Wang Yi, Wang Xiangyun. On the Preparation of Disodium Salt of Dodecahydrododecaborate[J]. Chinese Journal of Applied Chemistry, 1998, 15(5): 111-112.
Citation: Wang Fuquan, Wang Yi, Wang Xiangyun. On the Preparation of Disodium Salt of Dodecahydrododecaborate[J]. Chinese Journal of Applied Chemistry, 1998, 15(5): 111-112.
English
On the Preparation of Disodium Salt of Dodecahydrododecaborate
Abstract:
An improved method for preparation of closo dodecaborate B12 H122- with yield of 89.8% is described. The improved reaction conditions and separation procedure of the product for thermal decomposition of B3H8- to B12 H122- in diglyme are given. The method is suitable for routine preparation.
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Key words:
- disodium dodecahydrododecaborate
- / synthesis
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