引用本文:
Gui Jie TIAN, Chuan Liang QIU, Zhe LIU, De Xin WANG. Short Synthesis of C-terminal Modified Peptides by a Series-connection Procedure[J]. Chinese Chemical Letters,
2005, 16(1): 31-34.
Citation: Gui Jie TIAN, Chuan Liang QIU, Zhe LIU, De Xin WANG. Short Synthesis of C-terminal Modified Peptides by a Series-connection Procedure[J]. Chinese Chemical Letters, 2005, 16(1): 31-34.
Citation: Gui Jie TIAN, Chuan Liang QIU, Zhe LIU, De Xin WANG. Short Synthesis of C-terminal Modified Peptides by a Series-connection Procedure[J]. Chinese Chemical Letters, 2005, 16(1): 31-34.
Short Synthesis of C-terminal Modified Peptides by a Series-connection Procedure
摘要:
Three peptide alcohols and four peptidyl N-akyl-amides were prepared by a series-connection procedure consisting of n-1 sequencial assembly on solid support followed by ammonolysis with glycinol, benzylamine or n-butylamine, and successive extractionelution through C-18 layer. All products were obtained from this procedure without further purification,in an overall yield of 75-86%.
English
Short Synthesis of C-terminal Modified Peptides by a Series-connection Procedure
Abstract:
Three peptide alcohols and four peptidyl N-akyl-amides were prepared by a series-connection procedure consisting of n-1 sequencial assembly on solid support followed by ammonolysis with glycinol, benzylamine or n-butylamine, and successive extractionelution through C-18 layer. All products were obtained from this procedure without further purification,in an overall yield of 75-86%.
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Key words:
- Ammonolysis
- / C-18 filtration
- / solid-phase synthesis.
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