引用本文:
Shou Xin LIU, Yan Lou GENG, Xia TIAN, Xiao Li ZHEN, Jian Rong HAN. Total Synthesis of N-Methylsansalvamide A[J]. Chinese Chemical Letters,
2006, 17(6): 761-764.
Citation: Shou Xin LIU, Yan Lou GENG, Xia TIAN, Xiao Li ZHEN, Jian Rong HAN. Total Synthesis of N-Methylsansalvamide A[J]. Chinese Chemical Letters, 2006, 17(6): 761-764.
Citation: Shou Xin LIU, Yan Lou GENG, Xia TIAN, Xiao Li ZHEN, Jian Rong HAN. Total Synthesis of N-Methylsansalvamide A[J]. Chinese Chemical Letters, 2006, 17(6): 761-764.
Total Synthesis of N-Methylsansalvamide A
摘要:
Total synthesis of N-methylsansalvamide A was accomplished in solution phase by a convergent approach. An N-Boc-tri-depsipepide 6 and a dipeptide ester 10 were prepared in the yield of 89% and 91%, respectively. Cyclization of the linear penta-depsipetide was achieved with PyBOP and DIPEA in DMF-CH2Cl2.
English
Total Synthesis of N-Methylsansalvamide A
Abstract:
Total synthesis of N-methylsansalvamide A was accomplished in solution phase by a convergent approach. An N-Boc-tri-depsipepide 6 and a dipeptide ester 10 were prepared in the yield of 89% and 91%, respectively. Cyclization of the linear penta-depsipetide was achieved with PyBOP and DIPEA in DMF-CH2Cl2.
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Key words:
- Synthesis
- / N-methylsansalvamide A
- / solution phase
- / cyclic depsipeptide
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