引用本文:
Ping AI, Jia Chuan LIU, Min ZI, Zhi Hua DENG, Zhi Hong YAN, Li Ming YUAN. Enantioseparation of Aminoglutethimide by High-speed Counter current Chromatography Using Carboxymethly-β-cyclodextrin as Chiral Selector[J]. Chinese Chemical Letters,
2006, 17(6): 787-790.
Citation: Ping AI, Jia Chuan LIU, Min ZI, Zhi Hua DENG, Zhi Hong YAN, Li Ming YUAN. Enantioseparation of Aminoglutethimide by High-speed Counter current Chromatography Using Carboxymethly-β-cyclodextrin as Chiral Selector[J]. Chinese Chemical Letters, 2006, 17(6): 787-790.
Citation: Ping AI, Jia Chuan LIU, Min ZI, Zhi Hua DENG, Zhi Hong YAN, Li Ming YUAN. Enantioseparation of Aminoglutethimide by High-speed Counter current Chromatography Using Carboxymethly-β-cyclodextrin as Chiral Selector[J]. Chinese Chemical Letters, 2006, 17(6): 787-790.
Enantioseparation of Aminoglutethimide by High-speed Counter current Chromatography Using Carboxymethly-β-cyclodextrin as Chiral Selector
摘要:
Enantioseparation of aminoglutethimide was performed by high-speed counter-current chromatography with a two-phase system composed of ethyl acetate: methanol: water=10:l:9.The lower phase contained 20 mmol/L of carboxymethly-β-cyclodextrin as chiral selector. The enantiomers were separated in 1.2 h and identified by chiral HPLC. This method was very efficient for the chiral preparative separation.
English
Enantioseparation of Aminoglutethimide by High-speed Counter current Chromatography Using Carboxymethly-β-cyclodextrin as Chiral Selector
Abstract:
Enantioseparation of aminoglutethimide was performed by high-speed counter-current chromatography with a two-phase system composed of ethyl acetate: methanol: water=10:l:9.The lower phase contained 20 mmol/L of carboxymethly-β-cyclodextrin as chiral selector. The enantiomers were separated in 1.2 h and identified by chiral HPLC. This method was very efficient for the chiral preparative separation.
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