引用本文:
Cheng Guo JIA, Yun Pu WANG, Han Yu FENG. A LOW-PRESSURE AND ONE-STEP METHOD FOR THE SYNTHESIS OF ALKYLIDYNETRICOBALT NONACARBONYL CLUSTERS:RCCo8（CO）9[J]. Chinese Chemical Letters,
1993, 4(2): 121-122.
Citation: Cheng Guo JIA, Yun Pu WANG, Han Yu FENG. A LOW-PRESSURE AND ONE-STEP METHOD FOR THE SYNTHESIS OF ALKYLIDYNETRICOBALT NONACARBONYL CLUSTERS:RCCo8（CO）9[J]. Chinese Chemical Letters, 1993, 4(2): 121-122.
Citation: Cheng Guo JIA, Yun Pu WANG, Han Yu FENG. A LOW-PRESSURE AND ONE-STEP METHOD FOR THE SYNTHESIS OF ALKYLIDYNETRICOBALT NONACARBONYL CLUSTERS:RCCo8（CO）9[J]. Chinese Chemical Letters, 1993, 4(2): 121-122.
A LOW-PRESSURE AND ONE-STEP METHOD FOR THE SYNTHESIS OF ALKYLIDYNETRICOBALT NONACARBONYL CLUSTERS:RCCo8（CO）9
摘要:
Metal clusters RCCoa（CO）9（R-H,C1,Br,CHa,Ph） were preparedin 18.8-57.3% yields from the reaction of cobalt(Ⅱ)salt and RCXa under mild PTC conditions(latm CO,25℃).The cobalt salt was reducedto Co（CO）4 in the presence of NaaS2O4.
English
A LOW-PRESSURE AND ONE-STEP METHOD FOR THE SYNTHESIS OF ALKYLIDYNETRICOBALT NONACARBONYL CLUSTERS:RCCo8（CO）9
Abstract:
Metal clusters RCCoa（CO）9（R-H,C1,Br,CHa,Ph） were preparedin 18.8-57.3% yields from the reaction of cobalt(Ⅱ)salt and RCXa under mild PTC conditions(latm CO,25℃).The cobalt salt was reducedto Co（CO）4 in the presence of NaaS2O4.
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