引用本文:
吕艳阳, 刘小玉, 曹俊. 四(对甲氧基苯基)卟啉钐(Ⅲ)配合物的合成及表征[J]. 应用化学,
2010, 27(6): 691-694.
doi:
10.3724/SP.J.1095.2010.90472
Citation: LV Yan-Yang, LIU Xiao-Yu, CAO Jun. Synthesis and Characterization of Tetra(p-methoxy-phenyl) Porphyrin and Its Samarium(Ⅲ) Complexes[J]. Chinese Journal of Applied Chemistry, 2010, 27(6): 691-694. doi: 10.3724/SP.J.1095.2010.90472
Citation: LV Yan-Yang, LIU Xiao-Yu, CAO Jun. Synthesis and Characterization of Tetra(p-methoxy-phenyl) Porphyrin and Its Samarium(Ⅲ) Complexes[J]. Chinese Journal of Applied Chemistry, 2010, 27(6): 691-694. doi: 10.3724/SP.J.1095.2010.90472
四(对甲氧基苯基)卟啉钐(Ⅲ)配合物的合成及表征
English
Synthesis and Characterization of Tetra(p-methoxy-phenyl) Porphyrin and Its Samarium(Ⅲ) Complexes
Abstract:
A new tetra(p-methoxy-phenyl) porphyrin Sm(Ⅲ) complex was obtained by the reaction of samarium chloride and tetra(p-methoxy-phenyl) porphyrin in THF in a yield of 62.4%.Besides the coordination reaction conditions,ligands and their complexes fluorescence properties were studied.Their structures were identified by UV-Vis,IR,1H NMR and elemental analysis,which show that Sm(Ⅲ) complex has been formed.The reaction conditions were simple and easy to operate.
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Key words:
- meso-tetra(p-methoxy-phenyl)porphyrin
- / samarium(Ⅲ)
- / synthesis
- / fluorescence spectral
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