A facile synthesis of a novel energetic surfactant 1-amino-3-dodecyl-1, 2, 3-triazolium nitrate

Xiao-Hui Zhao Zhi-Wen Ye

Citation:  Xiao-Hui Zhao, Zhi-Wen Ye. A facile synthesis of a novel energetic surfactant 1-amino-3-dodecyl-1, 2, 3-triazolium nitrate[J]. Chinese Chemical Letters, 2014, 25(2): 209-211. shu

A facile synthesis of a novel energetic surfactant 1-amino-3-dodecyl-1, 2, 3-triazolium nitrate

    通讯作者: Zhi-Wen Ye,
摘要: 1-Amino-3-dodecyl-1,2,3-triazolium nitrate, as a novel energetic surfactant, has been synthesized in four steps, namely addition-elimination, cyclization, alkylation and metathesis. Its structure was confirmed by 1H NMR, IR, and MS. The effects of various reaction parameters, including stoichiometry, reaction temperature and time, were investigated in details. In addition, the physical and chemical properties of this energetic surfactant were measured.

English

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    1. [1] J.W. Guo, X. Zhong, H. Zhu, L.J. Feng, Y.D. Cui, Synthesis of novel quaternary ammonium surfactants containing adamantane, Chin. Chem. Lett. 23 (2012) 653-656.[1] J.W. Guo, X. Zhong, H. Zhu, L.J. Feng, Y.D. Cui, Synthesis of novel quaternary ammonium surfactants containing adamantane, Chin. Chem. Lett. 23 (2012) 653-656.

    2. [2] X.M. Ran, X. Guo, J.T. Ding, Plasmid DNA induces dodecyl triethyl ammonium bromide to aggregate into vesicle, Chin. Chem. Lett. 23 (2012) 1396-1398.[2] X.M. Ran, X. Guo, J.T. Ding, Plasmid DNA induces dodecyl triethyl ammonium bromide to aggregate into vesicle, Chin. Chem. Lett. 23 (2012) 1396-1398.

    3. [3] T. Geng, X.G. Teng, Q.X. Li, Y.J. Jiang, G.J. Li, Synthesis and properties of long-chain quaternary ammonium hydroxides, Chin. Chem. Lett. 24 (2013) 494-496.[3] T. Geng, X.G. Teng, Q.X. Li, Y.J. Jiang, G.J. Li, Synthesis and properties of long-chain quaternary ammonium hydroxides, Chin. Chem. Lett. 24 (2013) 494-496.

    4. [4] H. Li, X. Guo, Vesicle formation between single-chained cationic surfactants and ribo-oligonucleotides, Chin. Chem. Lett. 24 (2013) 82-84.[4] H. Li, X. Guo, Vesicle formation between single-chained cationic surfactants and ribo-oligonucleotides, Chin. Chem. Lett. 24 (2013) 82-84.

    5. [5] Z.Q. Xia, S.P. Chen, Q. Wei, C.F. Qiao, Syntheses and characterization of energetic compounds constructed from alkaline earth metal cations (Sr and Ba) and 1,2- bis(tetrazol-5-yl)ethane, J. Solid State Chem. 184 (2011) 1777-1783.[5] Z.Q. Xia, S.P. Chen, Q. Wei, C.F. Qiao, Syntheses and characterization of energetic compounds constructed from alkaline earth metal cations (Sr and Ba) and 1,2- bis(tetrazol-5-yl)ethane, J. Solid State Chem. 184 (2011) 1777-1783.

    6. [6] M.J. Rosen, Z.H. Zhu, T. Gao, Synergism in binary mixture of surfactants: 11. Mixtures containing mono- and disulfonated alkyl- and dialkyldiphenylethers, J. Colloid Interface Sci. 157 (1993) 254-259.[6] M.J. Rosen, Z.H. Zhu, T. Gao, Synergism in binary mixture of surfactants: 11. Mixtures containing mono- and disulfonated alkyl- and dialkyldiphenylethers, J. Colloid Interface Sci. 157 (1993) 254-259.

    7. [7] Y. Dong, Y. Jin, D.Q. Wei, Surface activity and solubilization of a novel series of functional polyurethane surfactants, Polym. Int. 56 (2007) 14-21.[7] Y. Dong, Y. Jin, D.Q. Wei, Surface activity and solubilization of a novel series of functional polyurethane surfactants, Polym. Int. 56 (2007) 14-21.

    8. [8] F.T. Wu, P. Liu, X.W. Ma, Tetrazole-1-acetic acid as a ligand for copper-catalyzed N-arylation of imidazoles with aryl iodides under mild conditions, Chin. Chem. Lett. 24 (2013) 893-896.[8] F.T. Wu, P. Liu, X.W. Ma, Tetrazole-1-acetic acid as a ligand for copper-catalyzed N-arylation of imidazoles with aryl iodides under mild conditions, Chin. Chem. Lett. 24 (2013) 893-896.

    9. [9] H. Xue, Y. Gao, B. Twamley, J.M. Shreeve, New energetic salts based on nitrogencontaining heterocycles, Chem. Mater. 17 (2005) 191-198.[9] H. Xue, Y. Gao, B. Twamley, J.M. Shreeve, New energetic salts based on nitrogencontaining heterocycles, Chem. Mater. 17 (2005) 191-198.

    10. [10] Y.G. Huang, H.X. Gao, B. Twamley, J.M. Shreeve, Highly dense nitranilates-containing nitrogen-rich cations, Chem.-A Eur. J. 15 (2009) 917-923.[10] Y.G. Huang, H.X. Gao, B. Twamley, J.M. Shreeve, Highly dense nitranilates-containing nitrogen-rich cations, Chem.-A Eur. J. 15 (2009) 917-923.

    11. [11] S. Daoud, T.R. Berger, M.J. Villeburn, Insensitive munition-type BNCP explosive material and methods for forming the same, USP8444784.[11] S. Daoud, T.R. Berger, M.J. Villeburn, Insensitive munition-type BNCP explosive material and methods for forming the same, USP8444784.

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  • 收稿日期:  2013-07-10
  • 网络出版日期:  2013-10-22
通讯作者: 陈斌, bchen63@163.com
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