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片层花状氧化镁的制备及其吸附性能研究

程文婷 ,  陈亚芬 ,  李扬 ,  程芳琴

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引用本文: 程文婷, 陈亚芬, 李扬, 程芳琴. 片层花状氧化镁的制备及其吸附性能研究[J]. 无机化学学报, 2013, 29(9): 1793-1798. doi: 10.3969/j.issn.1001-4861.2013.00.250 shu
Citation:  CHENG Wen-Ting, CHEN Ya-Fen, LI Yang, CHENG Fang-Qin. Preparation and Adsorption Capacity of Flower-Like Magnesium Oxide[J]. Chinese Journal of Inorganic Chemistry, 2013, 29(9): 1793-1798. doi: 10.3969/j.issn.1001-4861.2013.00.250 shu

片层花状氧化镁的制备及其吸附性能研究

  • 基金项目:

    国家国际科技合作专项项目(No.2012DFA91500) (No.2012DFA91500)

    高等学校博士学科点专向科研基金资助课题(No.20121401120012) (No.20121401120012)

    山西省环保厅环保科研课题(No.2012H08)资助项目。 (No.2012H08)

摘要: 本文以十六烷基三甲基溴化铵(CTAB)作为结构导向剂,利用尿素在高温条件下受热分解生成的二氧化碳与氯化镁反应,通过层-层自组装制备出具有片层花状结构的氧化镁,并以其对含Pb(Ⅱ)溶液的吸附为探针反应,研究其对重金属离子的吸附性能。实验结果表明,所制备氧化镁的前驱体为碱式碳酸镁;经过600℃焙烧后,得到的片层花状氧化镁比表面积大于60 m2·g-1,具有良好的吸附性能;对含Pb(II)溶液的吸附过程符合Langmuir等温吸附,最大吸附量达到320 mg·g-1。

English

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  • 收稿日期:  2013-01-10
  • 网络出版日期:  2013-03-21
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