一维链状锌配位聚合物{[Zn(H2O)2(L)(phen)]·3H2O}n的合成、晶体结构和性能研究

储召华 解庆范 陈延民

引用本文: 储召华, 解庆范, 陈延民. 一维链状锌配位聚合物{[Zn(H2O)2(L)(phen)]·3H2O}n的合成、晶体结构和性能研究[J]. 无机化学学报, 2013, 29(9): 1893-1896. doi: 10.3969/j.issn.1001-4861.2013.00.222 shu
Citation:  CHU Zhao-Hua, XIE Qing-Fan, CHEN Yan-Min. Synthesis, Crystal Structures and Properties of 1D Zinc(Ⅱ) Coordination Polymer {[Zn(H2O)2(L)(phen)]·3H2O}n[J]. Chinese Journal of Inorganic Chemistry, 2013, 29(9): 1893-1896. doi: 10.3969/j.issn.1001-4861.2013.00.222 shu

一维链状锌配位聚合物{[Zn(H2O)2(L)(phen)]·3H2O}n的合成、晶体结构和性能研究

  • 基金项目:

    广东省科技厅科技项目(No.2011B090400521) (No.2011B090400521)

    福建省科技厅科技项目(No.2008F5053)资助项目。 (No.2008F5053)

摘要: 合成了一种锌配位聚合物{[Zn(H2O)2(L)(phen)]·3H2O}n (1),其中,H2L=1-氨基-8-萘酚-3,6-二磺酸并利用元素分析、红外、紫外、荧光、热重和X-射线单晶衍射分析进行了表征。标题配合物属正交晶系,Pnma空间群,a=1.698 90(12) nm,b=0.661 88(11) nm,c=2.480 40(14) nm,V=2.789 1(5) nm3,Z=4,Mr=634.92,Dc=1.512 g·cm-3,R=0.058 6,wR=0.121 4。标题配合物呈现一维链状结构,链内L2-和phen配体之间存在π-π堆积作用,链与链之间通过氢键扩展为二维超分子网络。

English

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  • 收稿日期:  2012-10-24
  • 网络出版日期:  2013-03-11
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