引用本文:
郑瑜, 谢伟文, 张琳娜, 傅桂香, 俞璐, 朱自莹. Na3Fe(C2O4)3·5H2O的热解过程和FAB-MS断裂规律[J]. 物理化学学报,
1994, 10(09): 774-778.
doi:
10.3866/PKU.WHXB19940902
Citation: Zheng Yu, Xie Wei-Wen, Zhang Lin-Na, Fu Gui-Xiang, Yu Lu, Zhu Zi-Ying. Thermal Decompositon Process and the Fragmentation Regularity of FAB-Mass Spectra of the Complex [Na3Fe(C2O4)3]·5H2O[J]. Acta Physico-Chimica Sinica, 1994, 10(09): 774-778. doi: 10.3866/PKU.WHXB19940902
Citation: Zheng Yu, Xie Wei-Wen, Zhang Lin-Na, Fu Gui-Xiang, Yu Lu, Zhu Zi-Ying. Thermal Decompositon Process and the Fragmentation Regularity of FAB-Mass Spectra of the Complex [Na3Fe(C2O4)3]·5H2O[J]. Acta Physico-Chimica Sinica, 1994, 10(09): 774-778. doi: 10.3866/PKU.WHXB19940902
Na3Fe(C2O4)3·5H2O的热解过程和FAB-MS断裂规律
English
Thermal Decompositon Process and the Fragmentation Regularity of FAB-Mass Spectra of the Complex [Na3Fe(C2O4)3]·5H2O
Abstract:
The thermal decomposition process of iron trisoxalato complex has been investigated by InSitu IR spectroscopy. The Products in gaseous and solid phases were analyzed and verified by gas chromatographic analysis (GC), differential thermal analysis (DTA), thermogravimetric analysis (TGA) and high temperature X-ray powder diffraction (HXRD) as well. The Fast Atom Bombaxdment (FAB) Mass Spectra of title complex were detected.
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Key words:
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In Situ IR spectroscopy
- / Thermal decomposition
- / DTA-TGA
- / FAB-Mass spectra
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