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白果形钨酸铅的可控合成及光致发光特性

王莉 ,  周元林 ,  李迎军

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引用本文: 王莉, 周元林, 李迎军. 白果形钨酸铅的可控合成及光致发光特性[J]. 无机化学学报, 2014, 30(4): 828-836. doi: 10.11862/CJIC.2014.099 shu
Citation:  WANG Li, ZHOU Yuan-Lin, LI Ying-Jun. Controlled Synthesis and Luminescence Properties of Ginkgo-Like PbWO4[J]. Chinese Journal of Inorganic Chemistry, 2014, 30(4): 828-836. doi: 10.11862/CJIC.2014.099 shu

白果形钨酸铅的可控合成及光致发光特性

    通讯作者: 周元林 zyl603@163.com
  • 基金项目:

    国家自然科学基金委员会-中国工程物理研究院联合基金(No.11176026)资助项目。 (No.11176026)

摘要: 以酒石酸钠为表面活性剂,采用直接沉淀法合成了白果形钨酸铅晶体,通过扫描电子显微镜(SEM)、X射线衍射(XRD)、能量散射仪(EDS)及荧光发射光谱(PL)对产物的结构和性质进行了表征。探讨了酒石酸钠对(004)晶面的抑制作用以及pH值和陈化温度对产物形貌的影响,结合晶体的内部结构提出了产物可能的形成机制。结果表明,陈化温度为30℃时,晶体形貌最为规整,PbWO4晶体在紫外光激发下展现出强的绿光发射,在pH=9时可达到最大的发光强度。

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  • 收稿日期:  2013-09-06
  • 网络出版日期:  2013-10-30
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