引用本文:
Jun Biao CHANG, Rui Yun GUO, Juan HE, Rong Feng CHEN. Synthesis of N6-Cyclopropy1-2,6-diamino-9 β-D-arabinofuranosylpurine[J]. Chinese Chemical Letters,
1999, 10(5): 357-360.
Citation: Jun Biao CHANG, Rui Yun GUO, Juan HE, Rong Feng CHEN. Synthesis of N6-Cyclopropy1-2,6-diamino-9 β-D-arabinofuranosylpurine[J]. Chinese Chemical Letters, 1999, 10(5): 357-360.
Citation: Jun Biao CHANG, Rui Yun GUO, Juan HE, Rong Feng CHEN. Synthesis of N6-Cyclopropy1-2,6-diamino-9 β-D-arabinofuranosylpurine[J]. Chinese Chemical Letters, 1999, 10(5): 357-360.
Synthesis of N6-Cyclopropy1-2,6-diamino-9 β-D-arabinofuranosylpurine
摘要:
Synthesis of N6-cvclopropyl-2,6-diamino-9 β-D-arabinofuranosyl-purine has been accomplished by treatment ailylated 2-amino-6-chloro-purine 4 with 2.3.5-tri-O-benzyl-β-D-arabinofuranosyl chloride 3 in the presence of molecular sieves follwed by reaction with cyclopropylamine and debenzyl reaction to give the β-anomeric nucleoside. The structures of all products were confirmed by UV. 1H-NMR and elemental analysis.
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关键词:
- Cyclopropylamine
- / arabinofuranose
- / purnie
English
Synthesis of N6-Cyclopropy1-2,6-diamino-9 β-D-arabinofuranosylpurine
Abstract:
Synthesis of N6-cvclopropyl-2,6-diamino-9 β-D-arabinofuranosyl-purine has been accomplished by treatment ailylated 2-amino-6-chloro-purine 4 with 2.3.5-tri-O-benzyl-β-D-arabinofuranosyl chloride 3 in the presence of molecular sieves follwed by reaction with cyclopropylamine and debenzyl reaction to give the β-anomeric nucleoside. The structures of all products were confirmed by UV. 1H-NMR and elemental analysis.
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Key words:
- Cyclopropylamine
- / arabinofuranose
- / purnie
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