引用本文:
Jian Hua YU, Yu Lai HU, Wen Fei TAN, Shi Yan YANG, Yuan Qi YIN. Synthesis and Structure of 1,2-O-(1-Aryl-1-Propylidene)-D-Mannitol[J]. Chinese Chemical Letters,
1997, 8(12): 1033-1036.
Citation: Jian Hua YU, Yu Lai HU, Wen Fei TAN, Shi Yan YANG, Yuan Qi YIN. Synthesis and Structure of 1,2-O-(1-Aryl-1-Propylidene)-D-Mannitol[J]. Chinese Chemical Letters, 1997, 8(12): 1033-1036.
Citation: Jian Hua YU, Yu Lai HU, Wen Fei TAN, Shi Yan YANG, Yuan Qi YIN. Synthesis and Structure of 1,2-O-(1-Aryl-1-Propylidene)-D-Mannitol[J]. Chinese Chemical Letters, 1997, 8(12): 1033-1036.
Synthesis and Structure of 1,2-O-(1-Aryl-1-Propylidene)-D-Mannitol
摘要:
A method for selective reaction of 1-aryl-propane-1-ones with 1,2-dihydroxy group of D-mannitol in the presence of ZnCl2-BF3.Et2O to 1,2-O-(1-aryl-1-propylidene)-D-mannitol (1-4) is described.The compounds were first reported and determined by IR,MS,1H-/13C-NMR spectra,among them the structure of 1 was further defined by X-ray diffraction.
English
Synthesis and Structure of 1,2-O-(1-Aryl-1-Propylidene)-D-Mannitol
Abstract:
A method for selective reaction of 1-aryl-propane-1-ones with 1,2-dihydroxy group of D-mannitol in the presence of ZnCl2-BF3.Et2O to 1,2-O-(1-aryl-1-propylidene)-D-mannitol (1-4) is described.The compounds were first reported and determined by IR,MS,1H-/13C-NMR spectra,among them the structure of 1 was further defined by X-ray diffraction.
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