引用本文:
Jie Ying WU, Yu Pang TIAN, Hoong Kun FUN, Boon Chuan YIP. SYNTHESIS AND CRYSTAL STRUCTURE FOR PALLADIUM(Ⅱ) DITHIOCARBIMATO COMPLEX[J]. Chinese Chemical Letters,
1996, 7(1): 87-88.
Citation: Jie Ying WU, Yu Pang TIAN, Hoong Kun FUN, Boon Chuan YIP. SYNTHESIS AND CRYSTAL STRUCTURE FOR PALLADIUM(Ⅱ) DITHIOCARBIMATO COMPLEX[J]. Chinese Chemical Letters, 1996, 7(1): 87-88.
Citation: Jie Ying WU, Yu Pang TIAN, Hoong Kun FUN, Boon Chuan YIP. SYNTHESIS AND CRYSTAL STRUCTURE FOR PALLADIUM(Ⅱ) DITHIOCARBIMATO COMPLEX[J]. Chinese Chemical Letters, 1996, 7(1): 87-88.
SYNTHESIS AND CRYSTAL STRUCTURE FOR PALLADIUM(Ⅱ) DITHIOCARBIMATO COMPLEX
摘要:
The title complex crystallized in space group P21/c with Z=2 in a unit cell of dimensions,a=9.811(1)Å,b=16.851(2)Å,c=15.855(3)Å;β=98.71(1)°, v=2591.0(6)Å3, Dc=1.225gcm-3,F(000)=1024,μ=0.55mm-1,R=0.0338,Rw=0.0631.The geometry of the Pd(Ⅱ)complex is square-planar configuration. The S2C=NPhNH2 group coordinated as asymmetric bidentate ligand forming a stable four member ring by chelation through the two sulphur atoms.
English
SYNTHESIS AND CRYSTAL STRUCTURE FOR PALLADIUM(Ⅱ) DITHIOCARBIMATO COMPLEX
Abstract:
The title complex crystallized in space group P21/c with Z=2 in a unit cell of dimensions,a=9.811(1)Å,b=16.851(2)Å,c=15.855(3)Å;β=98.71(1)°, v=2591.0(6)Å3, Dc=1.225gcm-3,F(000)=1024,μ=0.55mm-1,R=0.0338,Rw=0.0631.The geometry of the Pd(Ⅱ)complex is square-planar configuration. The S2C=NPhNH2 group coordinated as asymmetric bidentate ligand forming a stable four member ring by chelation through the two sulphur atoms.
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