引用本文:
Ai Lian ZHENG, Yuan Lia WU. A NEW SYNTHETIC ROUTE TO α-DAMASOONE[J]. Chinese Chemical Letters,
1992, 3(3): 177-178.
Citation: Ai Lian ZHENG, Yuan Lia WU. A NEW SYNTHETIC ROUTE TO α-DAMASOONE[J]. Chinese Chemical Letters, 1992, 3(3): 177-178.
Citation: Ai Lian ZHENG, Yuan Lia WU. A NEW SYNTHETIC ROUTE TO α-DAMASOONE[J]. Chinese Chemical Letters, 1992, 3(3): 177-178.
A NEW SYNTHETIC ROUTE TO α-DAMASOONE
摘要:
A new synthetic route to α-damascone (4) starting from citral is described-The synthesis features allylatioa of α-cyclocitral (1) with allylic bromide in the presence of tin powder to give the crucial intermediate 1-(2',6',6'-trimethylcyclo-hexen-2'-yl)-3-buten-1-ol (2a) and (2b) in a combined yield of 70%.
English
A NEW SYNTHETIC ROUTE TO α-DAMASOONE
Abstract:
A new synthetic route to α-damascone (4) starting from citral is described-The synthesis features allylatioa of α-cyclocitral (1) with allylic bromide in the presence of tin powder to give the crucial intermediate 1-(2',6',6'-trimethylcyclo-hexen-2'-yl)-3-buten-1-ol (2a) and (2b) in a combined yield of 70%.
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