引用本文:
高竹林, 殷彩霞, 李全, 刘复初, 朱洪友. 南部松小蠹集合信息素(±)-Frontalin的合成[J]. 应用化学,
2001, 18(7): 589-591.
Citation: GAO Zhu-Lin, YIN Cai-Xi, LI Quan, LIU Fu-Chu, ZHU Hong-You. Synthesis of (±)-Frontalin, an Aggregation Pheromone of Bark Beetle[J]. Chinese Journal of Applied Chemistry, 2001, 18(7): 589-591.
Citation: GAO Zhu-Lin, YIN Cai-Xi, LI Quan, LIU Fu-Chu, ZHU Hong-You. Synthesis of (±)-Frontalin, an Aggregation Pheromone of Bark Beetle[J]. Chinese Journal of Applied Chemistry, 2001, 18(7): 589-591.
南部松小蠹集合信息素(±)-Frontalin的合成
English
Synthesis of (±)-Frontalin, an Aggregation Pheromone of Bark Beetle
Abstract:
(±)-Frontalin (1,5-dimethyl-6,8-dioxabicycl octane), an aggregation pheromone of bark beetle, was prepared from cyclohexanone via a key intermediate 6-hepten-2-one prepared by catalytic decarbonylation of 7-oxo-octanoic acid with acetic anhydride using palladium(Ⅱ) complex as catalyst.The structures of all the compounds were confirmed by IR, MS, 1H NMR and 13C NMR.
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Key words:
- dendroctonus frontalis
- / aggregation pheromone
- / frontalin
- / synthesis
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